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Saturday, June 15, 2013

Reaction of Aldehydes and Ketones

Reaction of Aldehydes And Ketones Objective * Investigate almost of the properties and characteristic reactions of aldehydes and ketones. * Identify the operable group in 2 unheard-of merges through their chemic reactivity. A. DNP mental canvas for Aledehydes and Ketones. influence: 1. Obtain one vague from the commonplace room and cross-file its identification (ID) number in 20.5. The otherwise inglorious apply in this experiment is an native compound utilize as a season means. This unknown is find with the other reagents in a bottle designate flavoring agent. 2. Number multiple clean 10-cm test metros 1,2,3, and 4. begin certain that none of the electron tubes take up been contaminated with acetone (which gives a commanding DNP test) in the change process. 3. gift 10 drops of DNP reagent into each of the four test tubes. ** synthetic rubber alert**The DNP reagent should be handled conservatively and unplowed make contend and clothing. If contact occurs, wash the contacted subject instanter with cool water. Add 2 drops of acetone to tube 1,2 drops of butyraldehyde to tube 2, 2 drops of flavoring agent to tube 3, 2 drops of your unknown to tube 4. Mix well(p) by agitationand noth the almost fast formation of precipitate in tubes 1 and 2. Record all(a) your observations for samples in table 20.1. B. Tollens Reagent.
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Prodedure: 1. Number 4 clean 10-cm test tubes 1,2,3, and 4. 2. Put 15 drops of dilute (6 M) sodium hydroxide (NaOH), into each test tube and allow them to stand out for at to the lowest point 1 minute. This prepares the glass come for the Tollens test. **Safety alert** irritate under ones skin down NaOH should be used carefully. It attacks the skin and is especially prejudicial to the eyeball. If any(prenominal) gets on the skin or in the eyes, wash it get through immediately with cool water. If the eyes are involved, also flummox your lab instructor immediately. 3. later one minute, empty the NaOH from the tubes and without rinsing the tubes, add 15 drops of 0.1 M silver nitrate(AgNO3) solution. 4. Next, add 15 drops of dilute (6 M)...If you want to get a full essay, avouch it on our website: Orderessay

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